Gas chromatography and mass spectrometry a practical guide /
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| Main Author: | |
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| Other Authors: | , |
| Format: | Electronic eBook |
| Language: | English |
| Published: |
Boston :
Elsevier,
2011.
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| Edition: | 2nd ed. |
| Subjects: | |
| Online Access: | An electronic book accessible through the World Wide Web; click to view |
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Table of Contents:
- The fundamentals of GC/MS
- Introduction and history
- Gas chromatography
- The gc/ms interface
- Mass spectrometry instrumentation
- Mass spectral data interpretation
- Quantitation with GC/MS
- GC conditions, derivatization, and mass spectral interpretation
- Of specific compound types
- Acids
- Alcohols
- Aldehydes
- Amides
- Amines
- Amino acid
- Common contaminants
- Drugs and their metabolites
- Esters
- Ethers
- Fluorinated compounds
- Gases
- Glycols
- Halogenated compounds (other than fluorinated)
- Hydrocarbons
- Isocyanates
- Ketones
- Nitriles
- Nitroaromatics
- Nitrogen-containing heterocyclics
- Nucleosides (TMS derivatives)
- Pesticides
- Phenols
- Phosphorus compounds
- Plasticizers and other polymer additives (including phthalates)
- Prostaglandins (MO-TMS derivatives)
- Solvents and their impurities
- Steroids
- Sugars (monosaccharides)
- Sulfur compounds
- Appendices
- A definitions of terms related to gas chromatography
- B definitions of terms related to mass spectrometry
- C atomic masses and isotope abundances
- X+1 and x+2 values for ions containing atoms of C and H based on
- Isotope contributions
- E isotope peak patterns for ions containing atoms of Cl and/or Br
- F steps to follow in the determination of an elemental composition
- Based on isotope peak intensity ratios
- G derivatization in GC/MS
- H points of comparison of LC/MS vs GC/MS
- I list of available EI mass spectral databases
- J information required for reporting a GC/MS analysis
- K third-party software for use with GC/MS
- GC installation and maintenance
- Troubleshooting common GC problems
- N maintenance, operating tips, and troubleshooting for mass spectrometers
- O mixtures for determining mass spectral resolution
- P cross-index chart for GC stationary phases
- Q ions for determining unknown structures.